What is the main use of 1,2-ethyldisulfonate disodium salt?
1,2-Dibutyl oxalate, its main use is also wide. In "Tiangong Kaiwu", this material can be used for dyeing and weaving.
In the ancient dye shop, if you want to get a fresh color, you often rely on various chemicals. 1,2-Dibutyl oxalate can be used as a mordant to help dyes fix on fabrics. The fabric is treated with it, and the color is more firm. Although it has been washed and exposed to the sun, it is not easy to fade. Cotton, linen and silk can be used to enhance color and retain color.
And in the fragrance industry, 1,2-dibutyl oxalate is also useful. The preparation of fragrances requires uniform dispersion of fragrances. This substance can be used as a dispersant to distribute the fragrances evenly in the substrate, and the aroma is more consistent and lasting. The incense made, either for incense to clean the room or for wearing incense, is of better quality due to the help of 1,2-dibutyl oxalate.
Furthermore, in some fine chemical processes, 1,2-dibutyl oxalate can be used as a solvent. Its solubility is good, allowing many insoluble substances to be uniformly dispersed in the system, which is convenient for chemical reactions or mixing and blending of substances. In the preparation of paints and inks, pigments, resins, etc. are often used to dissolve, the texture of the finished product is uniform, the application and printing are smooth, and the effect is delicate.
What are the physical properties of 1,2-ethyldisulfonate disodium salt?
1% 2C2-dibutyl oxalate is an organic compound. It has the following physical properties:
In appearance, it is mostly a colorless and transparent oily liquid under normal conditions, with a pure and uniform texture and no visible impurities. Looking at it, it looks like a clear oil, and under light, it can appear crystal clear.
In terms of smell, it emits a weak and special aromatic smell. This smell is not pungent, relatively mild, and can be faintly smelled at a certain distance, giving people a feeling of freshness.
Solubility is quite important. It is difficult to dissolve in water, and can form obvious stratification in water. Because its density is slightly lower than that of water, it floats on the surface of the water. But it can be well miscible with many organic solvents such as ethanol and ether. Just like mixing it with ethanol, the two can quickly blend to form a uniform solution.
The boiling point is about 245-246 ° C. When it is heated to this temperature range, 1% 2C2-dibutyl oxalate will convert from liquid to gaseous and begin to boil.
The melting point is about -31 ° C. Below this temperature, it will solidify from liquid to solid, just as water freezes when cold.
The density is about 0.986g/cm ³, which is slightly smaller than the density of water of 1g/cm ³, which is why it floats in the upper layer of water. The physical properties of
1% 2C2-dibutyl oxalate make it a very important organic compound with specific applications in many fields such as organic synthesis and fragrance preparation.
Is the chemical property of 1,2-ethyldisulfonate disodium salt stable?
The chemical properties of 1% 2C2-dibenzyl acetoxalate are still stable. In this compound, the structural interaction between the benzyl ester group and the acetylglycolic acid makes the molecular structure stable.
From the perspective of the characteristics of its chemical bonds, the conjugated system of the benzene ring in the benzyl ester group can disperse the electron cloud density, making the ester group connected to it more stable and less susceptible to attack by general chemical reagents. And the interaction between the acetyl group and the oxalic acid residue also contributes to the stability of the whole molecule.
Under normal conditions, such as room temperature and pressure, in a non-strong oxidizing, non-strong acidic or strong alkaline environment, this compound can maintain its chemical structure integrity. However, in case of strong acid and alkali, its ester structure may be hydrolyzed, thus changing its chemical properties. And if placed under extreme conditions of high temperature and aerobic, it may cause oxidation reactions, resulting in structural changes.
But overall, in the conventional experimental and storage environment, the chemical properties of 1% 2C2-dibenzyl acetooxalate are quite stable, and its inherent chemical structure and characteristics can be maintained for a long time.
What are the precautions for the storage and transportation of 1,2-ethyldisulfonate disodium salt?
1% 2C2-dibutyl oxalate is an organic compound. When storing and transporting, the following numbers should be paid attention to:
First, the storage place should be cool and well ventilated. Because of its flammability, if stored in a high temperature or poorly ventilated place, it is easy to cause fire in case of fire and endanger safety. "Tiangong Kaiwu" also goes: "Where things are hidden, it is advisable to choose a cool and common place to prevent them from changing." This is the general rule for the storage of things, and 1% 2C2-dibutyl oxalate is no exception.
Second, it needs to be stored separately from oxidants, acids, etc. When 1% 2C2-dibutyl oxalate comes into contact with oxidants, it is easy to cause violent chemical reactions, and even cause explosions; when coexisted with acids, it may affect their chemical properties and cause deterioration. Ancient books discuss the compatibility of objects, and it is often said that different species should avoid each other to prevent accidents. The same is true.
Third, the storage container must be tightly sealed. 1% 2C2-dibutyl oxalate is volatile. If the container is not well sealed, it will evaporate into the air, which will cause material loss on the one hand, and the volatile gas may be harmful to the environment and human health on the other. As Gu Yun said: "If you hide objects, you must strictly seal them to prevent gas leakage."
Fourth, during transportation, the vehicle should be equipped with a grounding device to prevent static electricity from causing danger. 1% 2C2-dibutyl oxalate is easy to generate static electricity due to shaking and other factors during transportation. If there is no grounding device to remove static electricity, static electricity will accumulate or cause fire and explosion. In the past, when people transported goods, they also knew that they were taking precautions against the micro. Today, when transporting 1% 2C2-dibutyl oxalate, they should pay more attention to the risk of static electricity.
Fifth, transport personnel should be professionally trained and familiar with the dangerous characteristics of 1% 2C2-dibutyl oxalate and emergency response methods. In case of emergencies, they can respond quickly and properly to reduce losses. In ancient times, the inheritance of craftsmen's skills and experience was still important. Today's transportation is related to safety, and the training of professionals is particularly important.
What is the production method of 1,2-ethyldisulfonate disodium salt?
The preparation method of 1% 2C2-dibutyl oxalate is as follows:
To prepare 1% 2C2-dibutyl oxalate, oxalic acid and n-butanol are often used as raw materials and obtained by esterification. This reaction requires the assistance of a catalyst, and concentrated sulfuric acid is a commonly used catalyst. The specific steps are as follows:
First take an appropriate amount of oxalic acid and n-butanol, and place it in a round-bottomed flask according to a certain amount of substance. Usually the amount of n-butanol will be slightly more than the theoretical amount to promote the fuller reaction of oxalic acid and increase the yield.
Next, carefully add an appropriate amount of concentrated sulfuric acid to the flask. In this reaction, concentrated sulfuric acid can not only be used as a catalyst to accelerate the process of esterification reaction, but also because of its water absorption, it can move the equilibrium of the reaction in the direction of ester formation. Caution should be taken when adding concentrated sulfuric acid, because it is highly corrosive and will emit a lot of heat when diluted.
Then, a reflux condensation device is installed on the flask. The purpose of this device is to make the evaporated steam during the reaction be condensed and refluxed into the flask to reduce the loss of raw materials and products and ensure that the reaction can continue.
Then place the round bottom flask on the heating device, slowly raise the temperature and maintain a certain temperature for heating. During the heating process, close attention should be paid to the change of temperature to prevent the occurrence of side reactions caused by excessive temperature and affect the purity of the product.
Wait for the reaction to reach a certain time, and after the reaction liquid cools, move it into the separation funnel. Wash with an appropriate amount of water first to remove impurities that are soluble in water, such as unreacted acids and catalysts. Then wash with a saturated sodium carbonate solution, which functions to further neutralize the residual acid and reduce the solubility of the ester, which is conducive to delamination.
After washing, the organic layer is separated, and then dried with a desiccant such as anhydrous magnesium sulfate to remove the remaining trace moisture.
Finally, by distillation, the fraction in a specific temperature range is collected, which is the pure 1% 2C2-dibutyl oxalate product.
Although there are many steps in this preparation method, each step is crucial, which is related to the purity and yield of the product. The experimenter needs to be careful to obtain satisfactory results.