What is the chemical structure of 4-Amino-1,1 '-Diphenylamine-2-Sulfonic Acid?
4 - Amino - 1,1 '- Diphenylamine - 2 - Sulfonic Acid, Chinese name 4 - amino - 1,1' - diphenylamine - 2 - sulfonic acid, its chemical properties are as follows.
This compound is mainly composed of benzene and nitrogen atoms, forming the basic framework of diphenylamine. In which the amino group of one benzene is connected to the position (1 - position) of the benzene, and another benzene is connected, this 1,1 '- diphenylamine part. On the other benzene, the amino group (-NH2O) is connected at the 2-position, and the sulfonic acid group (-SO-H) is connected at the position of the amino phase, that is, it forms a complete solution of 4-amino-1,1 '-diphenylamine-2-sulfonic acid.
Its chemical formula can be C-H-N-O-S, and the molecular weight of the phase is 264.30. This compound has specific uses in chemical reactions and some applications such as dyes and analysis. The sulfonic acid group can provide acidity, which is advantageous for its decomposition under specific conditions and for some molecular crossings; the amino group can be substituted and combined with some nuclei, making it important in the synthesis and phase domains.
What are the main uses of 4-Amino-1,1 '-Diphenylamine-2-Sulfonic Acid?
4-Amino-1,1 '-diphenylamine-2-sulfonic acid, with a crystalline powder and a light purple color, is often used as an indicator for analytical chemistry experiments.
This agent is widely used in the field of redox titration. Because of the specific chemical environment, its color becomes acute, which can indicate the end point of titration. In the experiment of potassium dichromate titration of ferrous ions, when ferrous ions are oxidized, the solution potential gradually changes, and at the end point, 4-amino-1,1 '-diphenylamine-2-sulfonic acid transiently changes from colorless to purplish-red. This significant color change allows the experimenter to accurately judge the end of the reaction, and the data measurement is more accurate.
Furthermore, it is also indispensable in the analysis process such as the determination of total iron in steel. First, iron is converted into a specific valence state with an appropriate reagent, and then titration is performed. 4-Amino-1,1 '-diphenylamine-2-sulfonic acid, with its characteristics, provides a clear label for the monitoring of the reaction process and the determination of the endpoint, and helps the experimenter obtain reliable analysis results. It is of great significance for the quality control and composition analysis of steel.
What are the physical properties of 4-Amino-1,1 '-Diphenylamine-2-Sulfonic Acid?
4-Amino-1,1 '-diphenylamine-2-sulfonic acid, in the form of purple-brown crystalline powder, soluble in water and ethanol. Its physical properties are particularly important and have a great impact on many chemical processes and industrial applications.
Looking at its properties, the purple-brown crystalline powder gives it a different appearance from others. In addition, it can be used as an important basis for identification and preliminary judgment.
In terms of solubility, it can be soluble in water and ethanol, which is of great significance. In aqueous systems, its solubility can participate in many chemical reactions, such as ion exchange, complexation reactions, etc. It can also be dissolved in organic solvents such as ethanol, which makes it suitable for use as a reaction intermediate or in the preparation of specific reaction solutions in the field of organic synthesis.
Furthermore, its melting point, boiling point and other data, although not detailed, are also key physical properties. The melting point is related to its physical state transition temperature. During the heating process, the melting point is changed from solid to liquid state. This temperature point is of important guiding value for its processing, molding and stability research in high temperature environments. The same is true for boiling points. Understanding boiling points helps to control its behavior in the gas phase environment and is a key reference indicator in separation operations such as distillation and fractionation.
In addition, the physical property of density is of great significance to the accurate measurement and the ratio of the reaction system. If a quantitative reaction is carried out and its density is known, the required quality can be accurately measured to ensure that the reaction is carried out according to the predetermined stoichiometric ratio, thereby improving the reaction efficiency and product purity.
The physical properties of 4-amino-1,1 '-diphenylamine-2-sulfonic acid, from appearance to solubility, to melting point, boiling point, density, etc., play an indispensable role in many aspects of chemical research and industrial production, and have far-reaching significance for in-depth exploration of its chemical behavior and expansion of its application range.
What is the synthesis method of 4-Amino-1,1 '-Diphenylamine-2-Sulfonic Acid?
The synthesis method of 4-amino-1,1 '-diphenylamine-2-sulfonic acid is as follows:
Take aniline first, and react with an appropriate amount of sulfuric acid to form aniline sulfate. This step requires attention to the amount of sulfuric acid and the reaction temperature. If the temperature is too high, side reactions will easily occur, resulting in impure products.
Then, aniline sulfate is heated to promote its isomerization, resulting in p-aminobenzenesulfonic acid. In this reaction process, the control of heating rate and time is very critical. If the rate is too fast or the time is too short, the isomerization will be incomplete; if the time is too long, it may cause an overreaction.
Then take p-aminobenzenesulfonic acid and carry out a condensation reaction with aniline under specific conditions In this step, a suitable catalyst needs to be selected, and the reaction temperature and reaction time are strictly controlled, so that the condensation reaction can proceed smoothly to generate 4-amino-1,1 '-diphenylamine-2-sulfonic acid.
After the reaction is completed, the product needs to be separated and purified. Crystallization, filtration, washing and other methods are often used to remove impurities and improve the purity of the product. After these steps, 4-amino-1,1' -diphenylamine-2-sulfonic acid can be obtained. During the synthesis process, precise control of the reaction conditions at each step is the key to obtaining high-purity products.
4-Amino-1,1 '-Diphenylamine-2-Sulfonic What are the precautions in the use of Acid
4-Amino-1,1 '-diphenylamine-2-sulfonic acid, when using, many matters need to be paid attention to.
First, this substance has certain toxicity and irritation, and should not be taken lightly when exposed. During operation, be sure to wear suitable protective equipment, such as protective gloves, goggles and gas masks, to prevent it from contacting the skin, eyes, or inhaling the human body through the respiratory tract, causing damage to the body.
Second, 4-amino-1,1' -diphenylamine-2-sulfonic acid is relatively sensitive to light and heat. When storing, it should be placed in a cool, dry and well-ventilated place, away from fire and heat sources, and at the same time avoid light to prevent it from deteriorating due to photothermal action and affecting the use effect.
Third, during use, precise control of the dosage is the key. It should be accurately weighed and added according to specific experimental requirements or production process regulations, and the dosage must not be increased or decreased at will. Too much dosage may not only cause waste, but also cause side reactions; if the dosage is too small, it will be difficult to achieve the desired effect.
Fourth, this substance acts as an indicator in some chemical reactions, and it is necessary to pay attention to the conditions of the reaction system when using it. For example, the pH of the solution has a great impact on its indication effect. The pH of the solution must be adjusted to an appropriate range according to the needs of the reaction to ensure that its indication effect is accurate.
Fifth, after use, the remaining substances must not be discarded at will. Relevant regulations must be followed and properly disposed of to prevent pollution to the environment. At the same time, the used utensils should also be cleaned in time to avoid residual substances affecting subsequent experiments or production.